Science of Synthesis

Science of Synthesis is the authoritative and comprehensive reference work for the entire field of organic and organometallic synthesis.

Science of Synthesis presents the important synthetic methods for all classes of compounds and includes:

Methods critically evaluated by leading scientists

Background information and detailed experimental procedures

Schemes and tables which illustrate the reaction scope

Preface

As our understanding of the natural world increases, we begin to understand complex phenomena at molecular levels. This level of understanding allows for the design of molecular entities for functions ranging from material science to biology. Such design requires synthesis and, as the structures increase in complexity as a necessity for specificity, puts increasing demands on the level of sophistication of the synthetic methods. Such needs stimulate the improvement of existing methods and, more importantly, the development of new methods. As scientists confront the synthetic problems posed by the molecular targets, they require access to a source of reliable synthetic information. Thus, the need for a new, comprehensive, and critical treatment of synthetic chemistry has become apparent. To meet this challenge, an entirely new edition of the esteemed reference work Houben-Weyl Methods of Organic Chemistry will be published starting in the year 2000.

To reflect the new broader need and focus, this new edition has a new title, Science of Synthesis, Houben-Weyl Methods of Molecular Transformations. Science of Synthesis will benefit from more than 90 years of experience and will continue the tradition of excellence in publishing synthetic chemistry reference works. Science of Synthesis will be a balanced and critical reference work produced by the collaborative efforts of chemists, from both industry and academia, selected by the editorial board. All published results from journals, books, and patent literature from the early 1800s until the year of publication will be considered by our authors, who are among the leading experts in their field. The 48 volumes of Science of Synthesis will provide chemists with the most reliable methods to solve their synthesis problems. Science of Synthesis will be updated periodically and will become a prime source of information for chemists in the 21st century.

Science of Synthesis will be organized in a logical hierarchical system based on the target molecule to be synthesized. The critical coverage of methods will be supported by information intended to help the user choose the most suitable method for their application, thus providing a strong foundation from which to develop a successful synthetic route. Within each category of product, illuminating background information such as history, nomenclature, structure, stability, reactivity, properties, safety, and environmental aspects will be discussed along with a detailed selection of reliable methods. Each method and variation will be accompanied by reaction schemes, tables of examples, experimental procedures, and a background discussion of the scope and limitations of the reaction described.

The policy of the editorial board is to make Science of Synthesis the ultimate tool for the synthetic chemist in the 21st century.

We would like to thank all of our authors for submitting contributions of such outstanding quality, and, also for the dedication and commitment they have shown throughout the entire editorial process.

October 2000

The Editorial Board

D. Bellus (Basel, Switzerland)

S. V. Ley (Cambridge, UK)

R. Noyori (Nagoya, Japan)

M. Regitz (Kaiserslautern, Germany)

P. J. Reider (New Jersey, USA)

E. Schaumann (Clausthal-Zellerfeld, Germany)

I. Shinkai (Tsukuba, Japan)

E. J. Thomas (Manchester, UK)

B. M. Trost (Stanford, USA)

Volume 10: Fused Five-Membered Hetarenes with One Heteroatom

Preface

Table of Contents

Introduction

E. J. Thomas

10.1 Product Class 1: Benzo[b]furans

C. P. Dell

10.2 Product Class 2: Benzo[c]furans

P. C. Steel

10.3 Product Class 3: Dibenzofurans

K. Jones

10.4 Product Class 4: Benzo[b]thiophenes

C. M. Rayner and M. A. Craham

10.5 Product Class 5: Benzo[c]thiophenes

T. L. Cilchrist and S. J. Higgins

10.6 Product Class 6: Dibenzothiophenes

M. D. Andrews

10.7 Product Class 7: Benzo[b]selenophenes

P. J. Murphy

10.8 Product Class 8: Benzo[c]selenophenes

P. J. Murphy

10.9 Product Class 9: Dibenzoselenophenes

P. J. Murphy

10.10 Product Class 10: Benzo[b]tellurophenes

P. J. Murphy

10.11 Product Class 11: Benzo[c]tellurophenes

P. J. Murphy

10.12 Product Class 12: Dibenzotellurophenes

P. J. Murphy

10.13 Product Class 13: Indole and Its Derivatives

J. A. Joule

10.14 Product Class 14: 1H- and 2H-Isoindoles

T. J. Donohoe

10.15 Product Class 15: Carbazoles

P. T. Callagher

10.16 Product Class 16: Indolizines

M. Shipman

10.17 Product Class 17: Benzo[b]phospholes

R. A. Aitken

10.18 Product Class 18: Benzo[c]phospholes

R. A. Aitken

10.19 Product Class 19: Dibenzophospholes

R. A. Aitken

10.20 Product Class 20: Phosphorus Analogues of Indolizines

R. A. Aitken

Keyword Index

Author Index

Abbreviations

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